منابع مشابه
Thin Layer Chromatographic Separation of Benzodiazepine Derivates
abstract: In this paper we describe the thin layer chromatographic separation of eight of the most frequently used benzodiazepine derivates (alprazolam, bromazepam, chlorazepate potassium, chlordiazepoxide, diazepam, nitrazepam, oxazepam) and their degradation products after acid hydrolysis. Our aim was not only to develop a simple, rapid and efficient method for their separation but also the o...
متن کاملQuantitative Thin-Layer Chromatographic Method for Determination of Amantadine Hydrochloride
A simple and accurate thin-layer chromatographic (TLC) method for quantitative determination of amantadine hydrochloride (AMD) was developed and validated. The method employed TLC aluminum plates pre-coated with silica gel 60F-254 as a stationary phase. The solvent system used for development consisted of n-hexane-methanol-diethylamine (80: 40: 5, v/v/v). The separated spots were visualized as ...
متن کاملThin layer chromatographic analysis of Beta-lactam antibiotics.
PURPOSE The paper describes some thin layer chromatographic procedures that allow simple and rapid separation and identification of penicillins and cephalosporins from complex mixtures. METHODS Using silicagel GF254 as stationary phase and selecting different mobile phases we succeeded in the separation of the studied beta-lactamins. Our aim was not only to develop a simple, rapid and efficie...
متن کاملThin-layer chromatographic technique for rapid detection of bacterial phospholipases.
Silica gel thin-layer chromatography was employed to detect lecithinase activity induced from bacterial resting cell preparations induced from bacterial resting cell preparations incubated at 37 C for 4 h in the presence of purified egg yolk lecithin. Bacillus subtilis, Bacillus cereus, Serratia marcescens, and Pseudomonas aeruginosa hydrolyzed lecithin with the formation of free fatty acids as...
متن کاملModeling of thin-layer chromatographic separation of androstane isomers
Modeling of thin-layer chromatographic separation of androstane isomers to find the optimum mobile phase is described in this paper. The isomers of androstane are present in a variety of samples, so achieving their optimum thin-layer chromatographic separation is very important. A mathematical model was developed and tested. The model takes into account the interaction between solvents and uses...
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ژورنال
عنوان ژورنال: Biochemical Journal
سال: 1972
ISSN: 0306-3283
DOI: 10.1042/bj1300058p